Mescaline

[Impman]

oohhhhhhh I seee the salt now.... I added the HCl Solution to the Xylene and watched carefully. It salts up pretty fucking good. .... I get it....... ok train back on the tracks

 

[Impman]

I wonder wtf that vaporization was all about!!!! I must have vaporized the mescaline too!! LOL

 

[Impman]

I can just see Mr.E Duck in my mind....slowly shaking his head reading my posts.... lol

 

[Impman]

got a little ball of resin from scrapping the pan... it looked like it would be dry salt...as I started to scrape it gooed up just like QWISO hash....it looks just like it too.......I think if I let it dry longer and slower it will be more crystally..... its only a tiny bit ..... 200 mg. I have more evaporating on the glass trey...

 

[MrEDuck]

I can just see Mr.E Duck in my mind....slowly shaking his head reading my posts.... lol

I have a sudden desire to have a drink with my old advisor.
What is the goo from? An evap test of the xylene?
Im worried I'm missing a step in your procedure, could you do me a favor and list out what you've done step by step? It'll make it easier for me to trouble shoot.

 

[Impman]

I added a couple pinches of citric acid to my 350ml of cactus tea. I phed and the ph is 4 or below. It is acidic.

I poured the 350 ml of cactus tea strained into a 1000ml separatory funnel.

I poured in 50 ml of Xylen and turned the funnel about 50 times. making sure to mix the xylene through the cactus tea.

I waited for the layers to seperate. Three layers formed. A top Xylene layer, a middle fat layer, and a bottom aceqeuos layer. I saved the bottom layer, and put the other two layers in a glass jar off to the side for disposal.

I poured the aceqeous layer back into the seperatory funnel. I then slowly added 100ml solution of sodium hydroxide. (ap. 30 grams of lye beads to 100 ml distilled water) I mixed the sodiumhydroxide sol and the acequous solution. I ph and the ph was 10 or above..... (my ph test is just a bottle of liquid that reacts with color to acid or base)

Now, I added 50 ml of Xylene to the seperatory funnel to mix with the tea( that is now mixed with sodium hydroxide solution and is basic) I mix the xylene and sodium hydro solution and waited for the emulsion layer to serperate. (took several minuts) Once the layers separated, I collected the sodium hydro solution and kept the Xylene(now containing the mescaline) in the seperatory funnel.

Now, I mix the dry ISO wit 19ml ISO to 1 ml of Muriatic Acid(HCl) .... Two layers form. I collect the bottom layer and leave the top layer (Xylene) in the seperatory funnel. -------when I do this a second time , adding HCl solution there is no seperation of the xylene and the solution.

With the bottom layer of HCl solution I let evaporate in a pyrex pan....it appears to be cloudy with what looks like tiny salt particles....then when it drys it looks like a white thin thin thin layer of pasty/salty stuff....When i scrape it, it changes color to a Qwiso resin looking shit that balls up just like qwiso.

 

[Impman]

I dont even care if I get to trip anymore.... I am patient as can be right now.... Im just chillen and trying to think..... balls



----=this post is a lie... i do want to trip

 

[MrEDuck]

That procedure should have worked. When you're dropping in the acidic IPA you should see xtals form. Maybe try it more concentrated but you should see an immediate unmistakable reaction when you add the acid.

 

[Impman]

I see the xtals ....they form slow like discs then they float to the bottom... the floating discs break apart into what looks like tiny snowflakes...or salt....... then I pour that onto the tray and I see the salty/cloudy liquid....maybe it was not dry enough? It was dry to the touch....just when I scraped the white/cloudy/crystal looking paste it instantly became this crazy Qwiso like substance... I have a ball of it that is about .4 grams.... errr 400 mg..... what is this ball? I smelled it and it kinda smells like cactus. maybe my fingers were dirty.... it does not smell like chemical anyways...


I have more on the glass pan drying. I just looked at it and it looks like salt in water. there looks to be 500 mg of salt. I will let it evaporate overnight. I think my impatience played a part there... I scrapped up the paste too soon....maybe it was crystalizing and if you have just a little moisture/ISO it will resin up like QWISO.............O

 

[Impman]

I evaporated 1ml of HCl in my home and it still smells like chemical..........not good...especially after I had to talk my wife back into my psyconautical exploration after 4th of July High Mescaline dose.....o boy

 

[Impman]

Dude...our government is burnt as fuck. Muriatic Acid is some fucking wild shit! My god it is strong, man! And they only sell it by the fucking gallon....... and yet I can't find 99% ISO or Xylene?!?!? jeebuz christo man....... Xylene is like sugar water compared to muriatic acid

 

[MrEDuck]

I told you you want ventilation. I used to work with TaCl5 which is vile stuff that breaks down to Ta2O5 and HCl on contact with moisture in the air. We threw a vial with residue we thought had been oxidized into the glass bucket during a cleanup and opened the bucket a few minutes later to a cloud of HCl. Thankfully it was next to a hood.

 

[Skuxx]

I think you lost us duck... what the hell is Tacl5. something pentachloride. Was that for the mdma days?

 

[Impman]

skuxx its probably fucking bad ass shit ,....In think.... ....bad ass shit..... i can see Skuxx and I smoking a blunt and watching Mr.E Duck through some glass window into his lab , while he finishes up the LSD.... oh and Skuxx and I have a line or two of Molly on a glass mirror..... maybe skuxx and rory can help....Ill just watch

 

[rory420420]

I do have minor chem under my educational belt,but ill bet id be on the other end of a line of molly...

 

[Impman]

yesssss....... so what IS this little ball of resin? It must be mescaline

 

[rory420420]

And what's this 'line or two bullshit?'...lol

 

[rory420420]

Post a pic bro!!

 

[Impman]

well, thats just what was left on the mirror ... the rest is in the briefcase.

I don't think we can watch the last part of the LSD anywho..... I remember Duck mentioning something about extreme light sensitivity and heat.... you can't look at the LSD funny during a certain stage .... LOL.... you need a hydropressurized molecular electron spinner and a silly hat to make LSD

pic comin, I have to charge the dohicky real quick

 

[MrEDuck]

I'm guessing there's some cactus gunk in it still. There's a reason you do a few pulls of defatting.
TaCl5 was something I worked with in R&D. I also worked in a lab you could look into. Even put a "Please Feed the Researchers" sign up.