Hash and Oil Picture Thread

[qwizoking]

Damn blu I can't believe nobody got back to ya

I would just smoke it by now.... especially if it burns right on your nail

 

[BluJayz]

Aright must be the nature of the beast. I did take a few hoots and it lost its berry taste; so that's disappointing.

 

[qwizoking]

I've found that light esters with a low boiling point make up much of that fruity taste....

Here http://www.leffingwell.com/chirality/acyclics.htm
Pretty awesome...

 

[BCOGYODA]

Hey Blu what temp did you get that oil up to during your vac?

 

[BCOGYODA]

This batch turned out beauty! The texture and consistency is sooooooo sweeeeet!

 

[Guzias1]

almosttttttt there...

p.s. i think im bringing my temps too high. gonna try and go lowwwww er

 

[Guzias1]

Aright must be the nature of the beast. I did take a few hoots and it lost its berry taste; so that's disappointing.

dayumm. but ya, what bc, what temps did you push? how long?> tanksss

 

[BCOGYODA]

dayumm. but ya, what bc, what temps did you push? how long?> tanksss

The last couple I haven't gone over 115 surface of wax temp. And I have them elevated in the chamber in a ramekin and the ramekin is on top of another ramekin. I think the wax likes not to be directly on the hot surface of the bottom of the chamber. But that's just a theory.
So I've gotten a few runs now to wax up at 115.

I'm purging longer now before I go in the vac chamber. I spray at night and just let the tane evap with no heat at all; just at room temp. When I get up in the morning there's only a couple bubbles and it's almost all just oil left in the pirex. Then I've been very low temp purging it on the griddle at 80F for a couple hours before going in the chamber. I keep whipping it around while it's on the griddle.

The muffin degassing takes awhile. Prob about an hour till it settles down then I put the oil to 100F and full vac purge like that for around 10 hrs or so I guess. Then I turn it up so the wax is 115F and it takes a few more hours it seems to wax up nicely. I check the temp every 45 min-1hr cause the griddle is set quite a bit warmer so the chamber likes to creeeeeep up in temp so I have to turn it down once in a while when the oil goes anything over 115 now.

I think it's a real safe temp. That batch I overheated and turned to perma goo was very costly so I wont be doing that again I hope. Gotta be sooooo careful with the temp!

 

[qwizoking]

Yea..your getting there....one day y'all will be at my level
The hotter it is the less efficient anything is..when decarbed at 500(your lighter) 50% or so makes it as intact thc when decarbed at 210 70% makes it as thc..when decarbed at 170 something like 81% when decarbed without heat its in the 90's

What I'm trying to say though is that every process works in this manner..never use heat to evap or purge and use as little heat as possible to smoke(vaporize).....

I do many processes that only marginally improve the product...add up a few marginal percentage points and after evap when its concentrated, collectively it makes for a far superior product............impatient people. And their heat! Lol

 

[MiG pilot]

The hotter it is the less efficient anything is.. when decarbed at 210 70% makes it as thc..when decarbed at 170 something like 81% when decarbed without heat its in the 90's

I do not think drying the extract under the fan and without heating, can be called "natural decarboxylation."
This process decarboxylates resin only in a very small degree if anything.
If the extract is still fragile, so it is not decarboxylated.

 

[qwizoking]

That reminds me....we have an ignore list

Lol studies have been done on thca and how fast it decarbs overtime.......so go argue with them
Russian troll




Id post up some studies.....but you still haven't read the last ones :/

 

[MiG pilot]

I do not think drying the extract under the fan and without heating, can be called "natural decarboxylation."
This process decarboxylates resin only in a very small degree if anything.
If the extract is still fragile, so it is not decarboxylated.

After such "natural decarboxylation" resin is brittle because is still in carboxyl form.
After the correct decarboxylation fragility gone and will never return.
The phenolic form does not crystallize.

 

[qwizoking]

Lol ..... i showed you patents describing crystallization under different circumstances using different techniques...it is crystallized for the purpose of the patents i showed you, in inhalers and nasal sprays...I've crystallized as well as thousands of other people doing it every day making certain thc products

I'm tired of all these fucking trolls..qwizo out for the day

Here is one just one off hand.. https://www.google.com/patents/EP2279735A2?cl=en

And yes in the process synthesizing thc none is thca..lol


I've found racemic powder upwards of 2/3 l-thc crystallizing at room temp........

 

[MiG pilot]

Thanks for the link, read on the first page -
[0006] Purified trans-(-)-Δ[SUP]9[/SUP]-THC is a thick, viscous, resinous material that has been compared to pine-tree sap and rubber cement.

Dipl. troll from the drugstore,
stop shitting next to my messages, please.

I am writing to calm people with no cognitive impairment,
Sadly you obviously do not meet this standard.

 

[qwizoking]

"In Internet slang, a troll (/ˈtroʊl/, /ˈtrɒl/) is a person who sows discord on the Internet by starting arguments or upsetting people, [1] by posting inflammatory, [2] extraneous, or off-topic messages in an online community (such as a forum, chat room, or blog), either accidentally [3][4] or with the deliberate intent of provoking readers into an emotional response [5] or of otherwise disrupting normal on-topic discussion."


So whats the crystalline racemic powder that's made??? Lol
Whatever...I have better things to do than argue with you about it..it can be done and is done everyday around the world

https://www.google.com/patents/EP2289509A2?cl=en

I have a few more.....and again it specifically states when synthesizing thc there is no thca that's not what were talking about

 

[MiG pilot]

So whats the crystalline racemic powder that's made??? Lol

Racemic? Wow!
If you're talking about a light yellow iso, untidy scraped on your avatar, it was undoubtedly THCA.

 

[qwizoking]

Do you even know an enantiomer is?
And do you read my posts?..I said multiple times not thca

And that white powder in my avatar was not scraped..razorblades are small...grabbing grams of it to another container gets messy, its a powder after all

Whoever told you it couldn't be crystallized was wrong, I'm sorry...almost anything no matter the shape or complexity of the mole cule can be crystallized..I know of very very few substances that can't and are all crazy long..actually just one that I know of....that doesn't mean its stable, you obviously have a lot of learning to do..and I apologize for allowing myself to succumb to my temper

 

[MiG pilot]

More current term is – graphomania (click here).

 

[sunni]

alrighty take an afk folks and go smoke a bowl!

 

[Guzias1]

back to the thread.... :]